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Palladium Catalysts [Cross-coupling Reaction using Transition Metal Catalysts]

The study of coupling reactions using organopalladium complexes has been advanced as well as that using organonickel complexes. Generally, the reactivity of organopalladium complexes is lower compared with organonickel complexes. However, they have higher chemical stability for oxidations and this makes them easy to use. Therefore, palladium complexes are most commonly used for cross-coupling reactions.

(1) Palladium complexes generally used in cross coupling reactions

Palladium-phosphine complexes are well used in cross-coupling reactions and commercially available. Pd(PPh3)4 and PdCl2(PPh3)2 are used without any treatment. Also, palladium catalysts are used prepared in situ from the precursors such as Pd(OAc)2 and Pd2(dba)3·CHCl3, with appropriate amounts of phosphines. When using divalent palladium complexes such as Pd(OAc)2, once they are reduced to zero-valent palladium species by some organometallic reagents, phosphines and amines, then their catalytic reactions can start.

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