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Synthesis of α-Diazoketones

No.135(July 2008)
I0643
(Isocyanoimino)triphenylphosphorane (1)
Compound 1 is a useful reagent for the synthesis of diazoketones. The compound 1 was reacted with acid chlorides followed by hydrolysis and then treated with triethylamine and a catalytic amount of p-toluenesulfonyl chloride to give diazoketones 2.1) Moreover, the compound 1 has been used for the synthesis of heterocyclic compounds 3 and 4.2)

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