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CAS RN: 78489-65-3 | Product Number: E1200
Ethyl α-Iodophenylacetate
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Purity: >97.0%(T)(HPLC)
Synonyms:
- α-Iodophenylacetic Acid Ethyl Ester
- Ethyl 2-Iodo-2-phenylacetate
- 2-Iodo-2-phenylacetic Acid Ethyl Ester
Product Documents:
| Size | Unit Price | Philadelphia, PA | Portland, OR | Japan* | Quantity |
|---|---|---|---|---|---|
| 5G |
$71.00
|
1 | Contact Us | 17 |
|
| 25G |
$214.00
|
Contact Us | 1 | 7 |
|
* Items in stock locally ship in 1-2 business days. Items from Japan stock are able to ship from a US warehouse within 2 weeks. Please contact TCI for lead times on items not in stock. Excludes regulated items and items that ship on ice.
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| Product Number | E1200 |
| Purity / Analysis Method | >97.0%(T)(HPLC) |
| Molecular Formula / Molecular Weight | C__1__0H__1__1IO__2 = 290.10 |
| Physical State (20 deg.C) | Liquid |
| Storage Temperature | Frozen (<0°C) |
| Condition to Avoid | Light Sensitive,Heat Sensitive |
| CAS RN | 78489-65-3 |
| Reaxys Registry Number | 6859197 |
| PubChem Substance ID | 354333819 |
Specifications
| Appearance | Light yellow to Brown clear liquid |
| Purity(HPLC) | min. 97.0 area% |
| Purity(Argentometric Titration) | min. 97.0 % |
Properties (reference)
| Flash point | 137 °C |
| Specific Gravity (20/20) | 1.57 |
| Refractive Index | 1.58 |
GHS
| Pictogram |
|
| Signal Word | Danger |
| Hazard Statements | H314 : Causes severe skin burns and eye damage. H290 : May be corrosive to metals. |
| Precautionary Statements | P501 : Dispose of contents/ container to an approved waste disposal plant. P234 : Keep only in original container. P264 : Wash skin thoroughly after handling. P280 : Wear protective gloves/ protective clothing/ eye protection/ face protection. P390 : Absorb spillage to prevent material damage. P303 + P361 + P353 : IF ON SKIN (or hair): Take off immediately all contaminated clothing. Rinse skin with water/shower. P301 + P330 + P331 : IF SWALLOWED: Rinse mouth. Do NOT induce vomiting. P363 : Wash contaminated clothing before reuse. P304 + P340 + P310 : IF INHALED: Remove person to fresh air and keep comfortable for breathing. Immediately call a POISON CENTER/doctor. P305 + P351 + P338 + P310 : IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. Immediately call a POISON CENTER/doctor. P406 : Store in corrosive resistant container with a resistant inner liner. P405 : Store locked up. |
Related Laws:
Transport Information:
| UN Number (DOT-AIR) | UN3265 |
| Class (DOT-AIR) | 8 |
| Packing Group (TCI-A) | II |
| HS Number | 2916.34.5500 |
Application
Alkyl Iodide Initiators for Organocatalyzed Living Radical Polymerization
General Scheme of Organocatalyzed Living Radical Polymerization1-4)
Goto et al. have reported that alkyl iodides are efficient initiators for organocatalyzed living radical polymerization which is a new family of living radical polymerization. Organic amines and organic salts are used as catalysts.1-4) Low polydispersity and metal free polymers can be obtained by using this method.
Ranges of Effective Alkyl Iodides in the Polymerizations of Methyl Methacrylate (MMA) and Butyl Acrylate (BA)1)
These alkyl iodides are effective initiators in methyl methacrylate (MMA) [M0087] and butyl acrylate (BA) [A0142] polymerizations using tributylmethylphosphonium iodide (BMPI) [M1455] or tetrabutylammonium iodide (BNI) [T0057] as a catalyst. Low-polydispersity polymers are obtainable.1)
References
- 1)a) L. Lei, M. Tanishima, A. Goto, H. Kaji, Y. Yamaguchi, H. Komatsu, T. Jitsukawa, M. Miyamoto, Macromolecules 2014, 47, 6610.
- b) A. Goto, T. Fukuda, Y. Tsujii, US 7399814, 2008.
- c) A. Goto, PCT Int. Appl. WO 2015122404, 2015.
- 2)A. Goto, A. Ohtsuki, H. Ohfuji, M. Tanishima, H. Kaji, J. Am. Chem. Soc. 2013, 135, 11131.
- 3)A. Ohtsuki, L. Lei, M. Tanishima, A. Goto, H. Kaji, J. Am. Chem. Soc. 2015, 137, 5610.
- 4)JP Patent No. 5850599, 5697026, 5881292, 5645165 and 5610402. JP Patent Appl. No. 2013-529906.
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