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CAS RN: 14070-51-0 | Product Number: C1674
N-Chlorosaccharin
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Purity: >96.0%(T)
Synonyms:
- 2-Chloro-1,2-benzisothiazol-3(2H)-one 1,1-Dioxide
Product Documents:
| Size | Unit Price | Philadelphia, PA | Portland, OR | Japan* | Quantity |
|---|---|---|---|---|---|
| 5G |
$94.00
|
1 | 1 | ≥40 |
|
| 25G |
$275.00
|
1 | 1 | 1 |
|
* Items in stock locally ship in 1-2 business days. Items from Japan stock are able to ship from a US warehouse within 2 weeks. Please contact TCI for lead times on items not in stock. Excludes regulated items and items that ship on ice.
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| Product Number | C1674 |
| Purity / Analysis Method | >96.0%(T) |
| Molecular Formula / Molecular Weight | C__7H__4ClNO__3S = 217.62 |
| Physical State (20 deg.C) | Solid |
| Storage Temperature | Refrigerated (0-10°C) |
| Condition to Avoid | Heat Sensitive |
| CAS RN | 14070-51-0 |
| Reaxys Registry Number | 177560 |
| PubChem Substance ID | 354334387 |
| MDL Number | MFCD00274277 |
Specifications
| Appearance | White to Almost white powder to crystaline |
| Purity(Iodometric Titration) | min. 96.0 % |
| Melting point | 145.0 to 152.0 °C |
Properties (reference)
| Melting Point | 148 °C |
| Solubility (soluble in) | Toluene |
GHS
| Pictogram |
|
| Signal Word | Warning |
| Hazard Statements | H315 : Causes skin irritation. H319 : Causes serious eye irritation. H351 : Suspected of causing cancer. |
| Precautionary Statements | P501 : Dispose of contents/ container to an approved waste disposal plant. P202 : Do not handle until all safety precautions have been read and understood. P201 : Obtain special instructions before use. P264 : Wash skin thoroughly after handling. P280 : Wear protective gloves/ protective clothing/ eye protection/ face protection. P308 + P313 : IF exposed or concerned: Get medical advice/ attention. P337 + P313 : If eye irritation persists: Get medical advice/ attention. P305 + P351 + P338 : IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. P302 + P352 : IF ON SKIN: Wash with plenty of soap and water. P332 + P313 : If skin irritation occurs: Get medical advice/ attention. P362 : Take off contaminated clothing and wash before reuse. P405 : Store locked up. |
Related Laws:
Transport Information:
| HS Number | 2925.19.4200 |
Application
N-Halosaccharin Usable for Halogenations
Experimental procedure: 1 (142 mg, 0.5 mmol) and LiClO4 (32 mg, 0.3 mmol) are dissolved in CH3CN (10 mL). The reaction mixture is stirred at room temperature for 15 min. N-Chlorosaccharin (0.55 mmol) is added and stirring is continued for an additional 30 min. After removal of the solvent, the residue is dissolved in CH2Cl2 (10 mL), washed with strd. aq. NaHCO3 (3 x 10 mL), dried over Na2SO4, filtered and the solvent is evaporated in vacuo. The solid is suspended in CH3OH (4 mL) and, to remove the unwanted saccharin, undissolved pure product is filtered to obtain 2 (148 mg, 93% yield).
References
- Highly regioselective halogenation of 1-phenyl-3-(3,5-dimethoxyphenyl)-propane-1,3-dione
PubMed Literature
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