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CAS RN: 51479-73-3 | Product Number: A2186
Allyl 2,2,2-Trichloroacetimidate

Purity: >98.0%(GC)
- 2,2,2-Trichloroacetimidic Acid Allyl Ester
Size | Unit Price | Philadelphia, PA | Portland, OR | Japan* | Quantity |
---|---|---|---|---|---|
5G |
$167.00
|
1 | Contact Us | 17 |
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Product Number | A2186 |
Purity / Analysis Method | >98.0%(GC) |
Molecular Formula / Molecular Weight | C__5H__6Cl__3NO = 202.46 |
Physical State (20 deg.C) | Liquid |
Storage Temperature | Refrigerated (0-10°C) |
Store Under Inert Gas | Store under inert gas |
Condition to Avoid | Moisture Sensitive,Heat Sensitive |
CAS RN | 51479-73-3 |
Reaxys Registry Number | 1907084 |
PubChem Substance ID | 125307218 |
MDL Number | MFCD00190710 |
Appearance | Colorless to Almost colorless clear liquid |
Purity(GC) | min. 98.0 % |
Boiling Point | 74 °C/11 mmHg |
Flash point | 74 °C |
Specific Gravity (20/20) | 1.34 |
Refractive Index | 1.49 |
Pictogram |
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Signal Word | Danger |
Hazard Statements | H315 : Causes skin irritation. H318 : Causes serious eye damage. H227 : Combustible liquid. |
Precautionary Statements | P501 : Dispose of contents/ container to an approved waste disposal plant. P210 : Keep away from heat/sparks/open flames/hot surfaces. No smoking. P264 : Wash skin thoroughly after handling. P280 : Wear protective gloves/ eye protection/ face protection. P370 + P378 : In case of fire: Use dry sand, dry chemical or alcohol-resistant foam to extinguish. P302 + P352 : IF ON SKIN: Wash with plenty of soap and water. P332 + P313 : If skin irritation occurs: Get medical advice/ attention. P362 : Take off contaminated clothing and wash before reuse. P305 + P351 + P338 + P310 : IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. Immediately call a POISON CENTER/doctor. P403 + P235 : Store in a well-ventilated place. Keep cool. |
HS Number | 2925.19.9100 |
A solution of allyl 2,2,2-trichloroacetimidate (2 mmol) in cyclohexane (2 mL) and subsequently BF3·Et2O (20 µL) are added to a stirred solution of the carboxylic acid (1 mmol) in CH2Cl2 (1 mL). After stirring at room temperature overnight the precipitated trichloroacetamide is removed by filtration. The filtrate is washed with 5% NaHCO3 aq., brine and then dried (Na2SO4). The solvent is evaporated under reduced pressure and the residue is purified by distillation or column chromatography using petroleum ether (40-60 °C) / EtOAc (9 : 1) as an eluent.
References
- 1) G. Kokotos, A. Chiou, Synthesis 1997, 168.
- 2) H. P. Wessel, T. Iversen, D. R. Bundle, J. Chem. Soc., Perkin Trans. 1 1985, 2247.
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