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CAS RN: 3282-30-2 | Product Number: P0677
Pivaloyl Chloride
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Purity: >98.0%(T)
Synonyms:
- 2,2-Dimethylpropionyl Chloride
- Trimethylacetyl Chloride
Product Documents:
| Size | Unit Price | Same Day | 2-3 Business Days | Other Lead Time |
Shipping Information
|
|---|---|---|---|---|---|
| 25ML |
NT$920
|
≥40 | 28 | It can be shipped in about 4-5 weeks after ordering | |
| 500ML |
NT$3,160
|
≥40 | ≥80 | It can be shipped in about 4-5 weeks after ordering |
* The above prices include freight cost, customs, and other charges to the destination except for products that need to be shipped by sea or dry ice. For details, please contact
our distributor
in Taiwan to order our product.
* The storage conditions are subject to change without notice.
| Product Number | P0677 |
| Purity / Analysis Method | >98.0%(T) |
| Molecular Formula / Molecular Weight | C__5H__9ClO = 120.58 |
| Physical State (20 deg.C) | Liquid |
| Storage Temperature | Refrigerated (0-10°C) |
| Store Under Inert Gas | Store under inert gas |
| Condition to Avoid | Moisture Sensitive,Heat Sensitive |
| CAS RN | 3282-30-2 |
| Reaxys Registry Number | 385668 |
| PubChem Substance ID | 125310048 |
| SDBS (AIST Spectral DB) | 2154 |
| MDL Number | MFCD00000709 |
Specifications
| Appearance | Colorless to Light yellow clear liquid |
| Purity(Argentometric Titration) | min. 98.0 % |
Properties (reference)
| Boiling Point | 106 °C |
| Flash point | 13 °C |
| Specific Gravity (20/20) | 0.99 |
| Refractive Index | 1.41 |
| Solubility (soluble in) | Ether, Acetone |
GHS
| Pictogram |
|
| Signal Word | Danger |
| Hazard Statements | H331 : Toxic if inhaled. H302 : Harmful if swallowed. H314 : Causes severe skin burns and eye damage. H402 : Harmful to aquatic life. H225 : Highly flammable liquid and vapor. H290 : May be corrosive to metals. |
| Precautionary Statements | P501 : Dispose of contents/ container to an approved waste disposal plant. P261 : Avoid breathing dust/ fume/ gas/ mist/ vapors/ spray. P273 : Avoid release to the environment. P270 : Do not eat, drink or smoke when using this product. P240 : Ground/bond container and receiving equipment. P210 : Keep away from heat/sparks/open flames/hot surfaces. No smoking. P233 : Keep container tightly closed. P234 : Keep only in original container. P243 : Take precautionary measures against static discharge. P241 : Use explosion-proof electrical/ ventilating/ lighting/ equipment. P242 : Use only non-sparking tools. P271 : Use only outdoors or in a well-ventilated area. P264 : Wash skin thoroughly after handling. P280 : Wear protective gloves/ protective clothing/ eye protection/ face protection. P370 + P378 : In case of fire: Use dry sand, dry chemical or alcohol-resistant foam to extinguish. P390 : Absorb spillage to prevent material damage. P303 + P361 + P353 : IF ON SKIN (or hair): Take off immediately all contaminated clothing. Rinse skin with water/shower. P301 + P330 + P331 : IF SWALLOWED: Rinse mouth. Do NOT induce vomiting. P363 : Wash contaminated clothing before reuse. P301 + P312 + P330 : IF SWALLOWED: Call a POISON CENTER/doctor if you feel unwell. Rinse mouth. P304 + P340 + P310 : IF INHALED: Remove person to fresh air and keep comfortable for breathing. Immediately call a POISON CENTER/doctor. P305 + P351 + P338 + P310 : IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. Immediately call a POISON CENTER/doctor. P403 + P233 : Store in a well-ventilated place. Keep container tightly closed. P403 + P235 : Store in a well-ventilated place. Keep cool. P406 : Store in corrosive resistant container with a resistant inner liner. P405 : Store locked up. |
Related Laws:
Transport Information:
| UN Number | UN2438 |
| Class | 6.1 / 3,8 |
| Packing Group | I |
| Air Transportation | Forbidden for Air Transport |
| H.S.code* | 2915.90-000 |
Application
Mild Chlorination of Alcohols
Typical Procedure (Chlorination of p-methoxybenzyl alcohol): A mixture of pivaloyl chloride (1.30 g, 10.86 mmol) and DMF (5 mL) is stirred at room temperature for 1 h. To the mixture is first added CH2Cl2 (25 mL) followed by alcohol (1 g, 7.24 mmol). The reaction is monitored (TLC) until the complete disappearance of starting material. Water (20 mL) is added, and then the organic phase is washed with 15 mL of a saturated solution of Na2CO3, followed by 1 N HCl and brine. The organic layers are dried over Na2SO4, and the solvent evaporated to yield p-methoxybenzyl chloride (0.91 g, 80%).
References
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