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CAS RN: 212333-72-7 | 产品编码: T2821
N,N,N',N'-Tetramethyl-S-(1-oxido-2-pyridyl)thiouronium Hexafluorophosphate
技术规格
Appearance | White to Almost white powder to crystal |
Purity(HPLC) | min. 98.0 area% |
Purity(with Total Nitrogen) | min. 98.0 % |
NMR | confirm to structure |
物性(参考值)
熔点 | 117 °C |
GHS
象形图 | |
信号词 | Warning |
危险性说明 | H315 : Causes skin irritation. H319 : Causes serious eye irritation. |
防范说明 | P264 : Wash skin thoroughly after handling. P280 : Wear protective gloves/ eye protection/ face protection. P302 + P352 : IF ON SKIN: Wash with plenty of water. P337 + P313 : If eye irritation persists: Get medical advice/ attention. P305 + P351 + P338 : IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. P362 + P364 : Take off contaminated clothing and wash it before reuse. P332 + P313 : If skin irritation occurs: Get medical advice/ attention. |
相关法规
运输信息
HS编码* | 2933.39-000 |
应用
Coupling Reagent
Typical Procedure: A solution of the carboxylic acid (1 mmol) and N,N,N',N'-tetramethyl-S-(1-oxido-2-pyridyl)thiouronium hexafluorophosphate (1 mmol) in DMF (10 mL) is stirred at room temperature for 30 min. The corresponding amine (1 mmol) is added, and the resulting mixture is stirred at room temperature for 4 h. sat. NaCl is added, and the mixture is extracted with AcOEt. The organic layers are washed with 2 N HCl, sat. NaHCO3 and water. The organics are dried (Na2SO4), filtered, and evaporated (15 Torr) affording the corresponding pure amides.
References
- Peptide coupling reagent
参考文献
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技术规格
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