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Published TCIMAIL newest issue No.197 | Notice of Discontinuing the Use of Password-Protected Compressed Files | Product Document Searching Made Easy by 2D Code! | TCI Life Science News December 2024 | [TCIPracticalExample] Reduction of Amide Group Using... | Various analytical charts can be searched on each product detail page and Product Document Search (The kinds of analytical charts differ by product)
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CAS RN: 73482-96-9 | 产品编码: R0161
Rhodium(II) Octanoate Dimer
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| 规格 | 单价 | 同一天 | 2-3个工作日 | 数量 |
|---|---|---|---|---|
| 200MG |
S$328.50
|
2 | 2 |
|
| 1G |
S$955.50
|
16 | 32 |
|
| 产品编码 | R0161 |
| 分子式/分子量 | C__3__2H__6__0O__8Rh__2 = 778.64 |
| 外观与形状（20°C） | 固体 |
| 储存温度 | 室温 (15°C以下阴凉干燥处) |
| 包装和容器 | 1G-Glass Bottle with Plastic Insert （查看图片）, 200MG-Glass Bottle with Plastic Insert （查看图片） |
| CAS RN | 73482-96-9 |
| Reaxys-RN | 14206645 |
| PubChem物质ID | 253662547 |
| MDL编号 | MFCD00064724 |
技术规格
| Appearance | Green to Dark green powder to crystal |
| Elemental analysis(Carbon) | 47.00 to 52.00 % |
物性（参考值）
GHS
相关法规
运输信息
| HS编码* | 2843.90-000 |
应用
An Intramolecular C-H Amination of Aryl Azides
Experimental procedure: to a mixture of 1 (0.056 g, 0.246 mmol), Rh2(O2CC7H15)4 (0.012 mmol) and 4A molecular sieves (0.056 g) is added 1,2-dichloroethane (0.2 mL). The resulting mixture is heated to 60 °C. After 16 h, the reaction mixture is cooled to room temperature, and the heterogenous mixture is filtered through SiO2. The filtrate is concentrated in vacuo. Purification by MPLC (EtOAc:hexanes = 0:100 – 5:95) affords 2 (0.034 g, 69% yield) as a white solid.
References
- Dirhodium(II)-Catalyzed Intramolecular C-H Amination of Aryl Azides
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