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CAS RN: 3140-73-6 | 产品编码: C1676
2-Chloro-4,6-dimethoxy-1,3,5-triazine
技术规格
Appearance | White to Almost white powder to crystal |
Purity(HPLC) | min. 97.0 area% |
Purity(Argentometric Titration) | min. 97.0 % |
Melting point | 76.0 to 80.0 °C |
物性(参考值)
熔点 | 78 °C |
沸点 | 100 °C/0.8 mmHg |
在水中的溶解度 | 3 g/l 25 °C |
GHS
象形图 | |
信号词 | Warning |
危险性说明 | H315 : Causes skin irritation. H319 : Causes serious eye irritation. |
防范说明 | P264 : Wash skin thoroughly after handling. P280 : Wear protective gloves/ eye protection/ face protection. P302 + P352 : IF ON SKIN: Wash with plenty of water. P337 + P313 : If eye irritation persists: Get medical advice/ attention. P305 + P351 + P338 : IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. P362 + P364 : Take off contaminated clothing and wash it before reuse. P332 + P313 : If skin irritation occurs: Get medical advice/ attention. |
相关法规
运输信息
HS编码* | 2933.69-000 |
应用
Condensing Agent
Experimental procedure: 1 (13.8 mmol), 2 (13.8 mmol), and CDMT (14.5 mmol) are mixed together. To the mixture is added acetonitrile (15 mL). The slurry is stirred and NMM (20.7 mmol) added over about 10 min. The slurry is stirred for 1-2 h. Water (50 mL) is added to the mixture, which initially dissolved the solids and then quickly generated a thick slurry as the product precipitated. The slurry is stirred for 1 h at room temperature, and the solids are isolated by filtration and washing with water (2 x 10 mL). 3 is isolated in 92% yield and >97% purity.
Reference
- New observations on peptide bond formation using CDMT
参考文献
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