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CAS RN: 10416-59-8 | Product Number: T0691
N,O-Bis(trimethylsilyl)acetamide Kit TMS-BA (25% in Acetonitrile) 1 mL × 8 / Reaction vial, capacity 2 mL × 8 [Trimethylsilylating Reagent, for NH2 compounds]
Purity:
Synonyms:
- TMS-BA Kit
- BSA Kit
Product Documents:
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Product Number | T0691 |
Physical State (20 deg.C) | Liquid |
Storage Temperature | Refrigerated (0-10°C) |
Store Under Inert Gas | Store under inert gas |
Condition to Avoid | Moisture Sensitive,Heat Sensitive |
Packaging and Container | 1KIT-Vial (View image) |
CAS RN | 10416-59-8 |
Reaxys Registry Number | 2206090 |
PubChem Substance ID | 87576562 |
MDL Number | MFCD00008270 |
Specifications
Appearance | Colorless to Light yellow clear liquid |
Effect test of TMS derivatization | Effective as derivatization agent DL-Threonine |
Properties (reference)
GHS
Pictogram | |
Signal Word | Danger |
Hazard Statements | H311 : Toxic in contact with skin. H302 + H332 : Harmful if swallowed or if inhaled. H315 : Causes skin irritation. H319 : Causes serious eye irritation. H370 : Causes damage to organs. H373 : May cause damage to organs through prolonged or repeated exposure. H225 : Highly flammable liquid and vapor. |
Precautionary Statements | P501 : Dispose of contents/ container to an approved waste disposal plant. P260 : Do not breathe dust/ fume/ gas/ mist/ vapors/ spray. P270 : Do not eat, drink or smoke when using this product. P240 : Ground/bond container and receiving equipment. P210 : Keep away from heat/sparks/open flames/hot surfaces. No smoking. P233 : Keep container tightly closed. P243 : Take precautionary measures against static discharge. P241 : Use explosion-proof electrical/ ventilating/ lighting/ equipment. P242 : Use only non-sparking tools. P271 : Use only outdoors or in a well-ventilated area. P264 : Wash skin thoroughly after handling. P280 : Wear protective gloves/ eye protection/ face protection. P370 + P378 : In case of fire: Use dry sand, dry chemical or alcohol-resistant foam to extinguish. P337 + P313 : If eye irritation persists: Get medical advice/ attention. P305 + P351 + P338 : IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. P308 + P311 : IF exposed or concerned: Call a POISON CENTER/doctor. P361 + P364 : Take off immediately all contaminated clothing and wash it before reuse. P303 + P361 + P353 : IF ON SKIN (or hair): Take off immediately all contaminated clothing. Rinse skin with water/shower. P332 + P313 : If skin irritation occurs: Get medical advice/ attention. P301 + P312 + P330 : IF SWALLOWED: Call a POISON CENTER/doctor if you feel unwell. Rinse mouth. P304 + P340 + P312 : IF INHALED: Remove person to fresh air and keep comfortable for breathing. Call a POISON CENTER/doctor if you feel unwell. P403 + P235 : Store in a well-ventilated place. Keep cool. P405 : Store locked up. |
Related Laws:
Transport Information:
UN Number | UN1992 |
Class | 3 / 6.1 |
Packing Group | II |
H.S.code* | 2931.90-000 |
Application
Trimethylsilylating Reagent for GC Derivatization
Experimental procedure: ca. 1 mg of sample and 1 mL of TMS-BA is placed into a dry vessel (about 2 mL of vial is preferable). After sealing the vessel, the reaction is proceeded by shaking or heating (e.g. for leucine, threonine, by heating for 15 min at 125 °C) to result a transparent solution. And then it is directly injected into GC.
References
- Quantitative gas-liquid chromatography of sulfur containing amino acids
Application
Reactivity of Trimethylsilylating Reagents : Trimethylsilylation of Alcohols
References
- Protection for the Hydroxyl Group, Including 1,2- and 1,3-Diols
- P. G. M. Wuts, in Greene’s Protective Groups in Organic Synthesis, 5th ed., ed. by P. G. M. Wuts, John Wiley & Sons, Inc., Hoboken, New Jersey, 2014, Chap. 2, 17.
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