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CAS RN: 16308-68-2 | Product Number: A2303
Allyl Phenyl Carbonate
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Purity: >98.0%(GC)
Synonyms:
- Carbonic Acid Allyl Phenyl Ester
Product Documents:
| Size | Unit Price | Same Day | 2-3 Business Days | Other Lead Time |
Shipping Information
|
|---|---|---|---|---|---|
| 5G |
$100.00
|
26 | 18 | It can be shipped in about 2 weeks after ordering | |
| 25G |
$262.00
|
11 | 26 | It can be shipped in about 2 weeks after ordering |
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| Product Number | A2303 |
| Purity / Analysis Method | >98.0%(GC) |
| Molecular Formula / Molecular Weight | C__1__0H__1__0O__3 = 178.19 |
| Physical State (20 deg.C) | Liquid |
| Storage Temperature | Room Temperature (Recommended in a cool and dark place, <15°C) |
| Store Under Inert Gas | Store under inert gas |
| Condition to Avoid | Air Sensitive |
| CAS RN | 16308-68-2 |
| Reaxys Registry Number | 3253031 |
| PubChem Substance ID | 125307508 |
| MDL Number | MFCD07784342 |
Specifications
| Appearance | Colorless to Almost colorless clear liquid |
| Purity(GC) | min. 98.0 % |
| NMR | confirm to structure |
Properties (reference)
| Boiling Point | 78 °C/0.2 mmHg |
| Specific Gravity (20/20) | 1.11 |
| Refractive Index | 1.50 |
GHS
| Pictogram |
|
| Signal Word | Warning |
| Hazard Statements | H319 : Causes serious eye irritation. |
| Precautionary Statements | P264 : Wash skin thoroughly after handling. P280 : Wear eye protection/ face protection. P337 + P313 : If eye irritation persists: Get medical advice/ attention. P305 + P351 + P338 : IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. |
Related Laws:
Transport Information:
| H.S.code* | 2920.90-000 |
Application
Mono Carbamate Protection of Aliphatic Diamines
Typical Procedure (Mono Carbamate Protection of Aliphatic Diamines): Allyl phenyl carbonate (10 mmol) is added to a stirring solution of diamine (5.0 mmol) in absolute EtOH (20 mL). The reaction mixture is stirred over night at room temperature followed by removal of the volatiles in vacuo. H2O (25 mL) is added and the pH adjusted to 3 by addition of aq. HCl (2 M) followed by extraction with CH2Cl2 (2 × 50 mL). The aq phase is then made strongly alkaline by addition of aq. NaOH (2 M) and extracted with CH2Cl2 (3 × 80 mL). The organic phase is dried (Na2SO4), filtered and concentrated in vacuo to afford the desired products.
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