Maximum quantity allowed is 999
Please select the quantity
CAS RN: 131-09-9 | Product Number: C0123
2-Chloroanthraquinone
×
![]()
×
Purity: >99.0%(GC)
Synonyms:
Product Documents:
| Size | Unit Price | Same Day | 2-3 Business Days | Other Lead Time |
Shipping Information
|
|---|---|---|---|---|---|
| 25G |
$33.00
|
38 | 3 | Contact Us |
* Please contact our distributors or
TCI
to order our products. The above prices do not include freight cost, customs, and other charges to the destination.
* The storage conditions are subject to change without notice.
| Product Number | C0123 |
| Purity / Analysis Method | >99.0%(GC) |
| Molecular Formula / Molecular Weight | C__1__4H__7ClO__2 = 242.66 |
| Physical State (20 deg.C) | Solid |
| Storage Temperature | Room Temperature (Recommended in a cool and dark place, <15°C) |
| CAS RN | 131-09-9 |
| Reaxys Registry Number | 2051842 |
| PubChem Substance ID | 87565303 |
| SDBS (AIST Spectral DB) | 122 |
| MDL Number | MFCD00001227 |
Specifications
| Appearance | White to Light orange to Yellow powder to crystal |
| Purity(GC) | min. 99.0 % |
| Melting point | 209.0 to 212.0 °C |
| NMR | confirm to structure |
Properties (reference)
| Melting Point | 210 °C |
| Boiling Point | 292 °C/30 mmHg |
| Solubility in water | Insoluble |
| Solubility (soluble in) | Ethanol, Benzene, Nitrobenzene |
GHS
| Pictogram |
|
| Signal Word | Warning |
| Hazard Statements | H302 : Harmful if swallowed. H315 : Causes skin irritation. H319 : Causes serious eye irritation. H412 : Harmful to aquatic life with long lasting effects. |
| Precautionary Statements | P501 : Dispose of contents/ container to an approved waste disposal plant. P273 : Avoid release to the environment. P270 : Do not eat, drink or smoke when using this product. P264 : Wash skin thoroughly after handling. P280 : Wear protective gloves/ eye protection/ face protection. P302 + P352 : IF ON SKIN: Wash with plenty of water. P337 + P313 : If eye irritation persists: Get medical advice/ attention. P305 + P351 + P338 : IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. P362 + P364 : Take off contaminated clothing and wash it before reuse. P332 + P313 : If skin irritation occurs: Get medical advice/ attention. P301 + P312 + P330 : IF SWALLOWED: Call a POISON CENTER/doctor if you feel unwell. Rinse mouth. |
Related Laws:
| RTECS# | CB6151000 |
Transport Information:
| H.S.code* | 2914.79-000 |
Application
Aerobic Photooxidative Carbon–Carbon Bond Formation between Tertiary Amines and Carbon Nucleophiles
Typical Procedure (Entry 1):
A solution of 2-phenyl-1,2,3,4-tetrahydroisoquinoline (0.3 mmol), 2-chloroanthraquinone (0.021 mmol) and MeNO2 (1.5 mmol) in MeOH (3 mL) in a Pyrex test tube, purged with an O2 balloon, is stirred and externally irradiated by fluorescent lamps for 20 h. The mixture is then concentrated in vacuo. Purification of the crude product by flash chromatography on silica gel (hexane : EtOAc : Et3N = 100 : 10 : 1) gives 1-(nitromethyl)-2-phenyl-1,2,3,4-tetrahydroisoquinoline (64.5 mg, Y. 80%).
A solution of 2-phenyl-1,2,3,4-tetrahydroisoquinoline (0.3 mmol), 2-chloroanthraquinone (0.021 mmol) and MeNO2 (1.5 mmol) in MeOH (3 mL) in a Pyrex test tube, purged with an O2 balloon, is stirred and externally irradiated by fluorescent lamps for 20 h. The mixture is then concentrated in vacuo. Purification of the crude product by flash chromatography on silica gel (hexane : EtOAc : Et3N = 100 : 10 : 1) gives 1-(nitromethyl)-2-phenyl-1,2,3,4-tetrahydroisoquinoline (64.5 mg, Y. 80%).
References
PubMed Literature
Articles/Brochures
Product Documents (Note: Some products will not have analytical charts available.)
Safety Data Sheet (SDS)
Please select Language.
The requested SDS is not available.
Please Contact Us for more information.
Specifications
C of A & Other Certificates
Please enter Lot Number
Incorrect Lot Number. Please input only the 4-5 alphanumeric characters before the hyphen.
Sample C of A
This is a sample C of A and may not represent a recently manufactured lot of the product.
A sample C of A for this product is not available at this time.
Analytical Charts
Please enter Lot Number
Incorrect Lot Number. Please input only the 4-5 alphanumeric characters before the hyphen.
The requested analytical chart is not available. Sorry for the inconvenience.