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CAS RN: 205319-10-4 | Product Number: D4333
Dichloro[9,9-dimethyl-4,5-bis(diphenylphosphino)xanthene]palladium(II)
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![Dichloro[9,9-dimethyl-4,5-bis(diphenylphosphino)xanthene]palladium(II)](/_ui/responsive/theme-tci/images/missing_product_zoom.jpg "Dichloro[9,9-dimethyl-4,5-bis(diphenylphosphino)xanthene]palladium(II)")
Purity: >98.0%(T)
Synonyms:
- [4,5-Bis(diphenylphosphino)-9,9-dimethylxanthene]dichloropalladium(II)
- [4,5-Bis(diphenylphosphino)-9,9-dimethylxanthene]palladium(II) Dichloride
- Pd(Xantphos)Cl2
Product Documents:
| Size | Unit Price | Saitama (Kawaguchi) | Hyogo (Amagasaki) | Stock in other WH |
Shipping Information
|
|---|---|---|---|---|---|
| 200MG |
¥3,600
|
22 | 10 | Contact Us | |
| 1G |
¥13,000
|
8 | 23 | 20 |
* Available Stock: Prompt shipment (for products) in Saitama/Hyogo warehouse. Stock In Other WH: Shipment in about 2-3 Business Days from Saitama warehouse. Please contact us
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* The displayed price is the unit price and does not include consumption tax. The unit prices displayed are the latest and are subject to change without notice.
* To send your quote request for bulk quantities, please click on the "Request Bulk Quote" button. Please note that we cannot offer bulk quantities for some products.
*TCI frequently reviews storage conditions to optimize them. Please note that the latest information on the storage temperature for the products is described on our website.
| Product Number | D4333 |
| Purity / Analysis Method | >98.0%(T) |
| Molecular Formula / Molecular Weight | C__3__9H__3__2Cl__2OP__2Pd = 755.95 |
| Physical State (20 deg.C) | Solid |
| Storage Temperature | Room Temperature (Recommended in a cool and dark place, <15°C) |
| Store Under Inert Gas | Store under inert gas |
| Condition to Avoid | Air Sensitive |
| Packaging and Container | 1G-Glass Bottle with Plastic Insert (View image), 200MG-Glass Bottle with Plastic Insert (View image) |
| CAS RN | 205319-10-4 |
| Reaxys Registry Number | 17620547 |
| PubChem Substance ID | 253659676 |
| MDL Number | MFCD14155707 |
Specifications
| Appearance | Light yellow to Brown powder to crystal |
| Purity(Chelometric Titration) | min. 97.0 % |
Properties (reference)
| Melting Point | 287 °C(dec.) |
GHS
Related Laws:
Transport Information:
Application
Synthesis of Arylacetamides via Benzylic C―H Bond Activation using a Palladium Catalyst
Typical Procedure:
A mixture of Pd(Xantphos)Cl2 (7.6 mg, 5 mol %), toluene derivative (20.0 mmol), amine (0.2 mmol) and TBP (53.0 mg, 0.36 mmol) is added into an autoclave. Then the autoclave is purged and charged with CO at 10 atm. The reaction mixture is stirred at 120 °C for 16 h, and then CO is carefully released. The corresponding reaction mixture is purified by flash column chromatography on silica gel to give the desired product.
A mixture of Pd(Xantphos)Cl2 (7.6 mg, 5 mol %), toluene derivative (20.0 mmol), amine (0.2 mmol) and TBP (53.0 mg, 0.36 mmol) is added into an autoclave. Then the autoclave is purged and charged with CO at 10 atm. The reaction mixture is stirred at 120 °C for 16 h, and then CO is carefully released. The corresponding reaction mixture is purified by flash column chromatography on silica gel to give the desired product.
References
PubMed Literature
Articles/Brochures
TCIMAIL
[TCIMAIL No.164] Useful Palladium Catalyst for C(sp3)–H Activation[Research Articles] Synthesis of Arylacetamides via Benzylic C-H Bond Activation using a Palladium Catalyst
Product Documents (Note: Some products will not have analytical charts available.)
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