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Metal-Free Fluorination of C(sp3)-H Bonds using a Catalytic N-Oxyl Radical

Inoue et al. have reported the metal-free fluorination of C(sp3)—H bonds using NDHPI and F-TEDA-BF4. According to their results, a catalytic N-oxyl radical generated from NDHPI extracts hydrogen from the C(sp3)—H bond, and the resulting carbon radical is trapped by F-TEDA-BF4 to form the C(sp3)—F bond. This protocol is useful for the synthesis of various fluorinated compounds because it enables the chemoselective introduction of a fluorine atom into various aromatic and aliphatic compounds.

D4413

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