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CAS RN: 912823-79-1 | 產品號碼: P1626
Pentafluoroanilinium Trifluoromethanesulfonate
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| 產品號碼 | P1626 |
| 純度/分析方法 | >98.0%(T)(HPLC) |
| 分子式 / 分子量 | C__7H__3F__8NO__3S = 333.15 |
| 外觀與形狀（20°C） | Solid |
| 儲存條件 | Room Temperature (Recommended in a cool and dark place, <15°C) |
| 包裝和容器 | 1G-Glass Bottle with Plastic Insert （閲覽圖片） |
| CAS RN | 912823-79-1 |
| Reaxys-RN | 15026764 |
| PubChem Substance ID | 87558623 |
產品規格
| Appearance | White to Light yellow to Dark green powder to crystal |
| Purity(HPLC) | min. 98.0 area% |
| Purity(Neutralization titration) | min. 98.0 % |
性質
| 水溶性 | Soluble |
GHS
| 圖形表示 |
|
| 信號詞 | Danger |
| 危險性說明 | H314 : Causes severe skin burns and eye damage. |
| 防範說明 | P501 : Dispose of contents/ container to an approved waste disposal plant. P260 : Do not breathe dusts or mists. P264 : Wash skin thoroughly after handling. P280 : Wear protective gloves/ protective clothing/ eye protection/ face protection. P303 + P361 + P353 : IF ON SKIN (or hair): Take off immediately all contaminated clothing. Rinse skin with water/shower. P301 + P330 + P331 : IF SWALLOWED: Rinse mouth. Do NOT induce vomiting. P363 : Wash contaminated clothing before reuse. P304 + P340 + P310 : IF INHALED: Remove person to fresh air and keep comfortable for breathing. Immediately call a POISON CENTER/doctor. P305 + P351 + P338 + P310 : IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. Immediately call a POISON CENTER/doctor. P405 : Store locked up. |
相關法規
運輸資料
| UN編號 | UN1759 |
| 類別 | 8 |
| 包裝類別 | III |
| HS編碼* | 2921.42-000 |
Application
Efficient Method for the Catalytic Esterification using Ammonium Triflate Catalyst
References
- Y. Tanabe, T. Misaki, H. Iida, Y. Arai, Yuki Gosei Kagaku Kyokaishi (J. Synth. Org. Chem., Jpn.) 2004, 62, 1249.
- T. Funatomi, K. Wakasugi, T. Misaki, Y. Tanabe, Green Chemistry, 2006, 8, 1022.
Application
Synthesis of Bis-indolyl Methane Derivatives Using PFPAT Catalyst
Typical Procedure:
A mixture of aldehyde (1 mmol), indole (2 mmol) dissolved in acetonitrile (3 mL), and PFPAT (10 mol%) is stirred for appropriate reaction time. The reaction is monitored by TLC. The organic phase is washed with 1 M NaOH aqueous solution (1 mL). The separated organic phase is evaporated under reduced pressure to give a crude product, which is purified by distillation or by column chromatography (hexane–ethyl acetate).
A mixture of aldehyde (1 mmol), indole (2 mmol) dissolved in acetonitrile (3 mL), and PFPAT (10 mol%) is stirred for appropriate reaction time. The reaction is monitored by TLC. The organic phase is washed with 1 M NaOH aqueous solution (1 mL). The separated organic phase is evaporated under reduced pressure to give a crude product, which is purified by distillation or by column chromatography (hexane–ethyl acetate).
References
考研文獻
TCIMail
[TCIMAIL No.138] Useful Ammonium Triflate Catalysts for Esterification[Research Articles] Synthesis of Bis-indolyl Methane Derivatives Using PFPAT Catalyst
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