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CAS RN: 17082-61-0 | Product Number: B1768
1,2-Bis(trimethylsilyloxy)cyclobutene
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Purity: >94.0%(GC)
Synonyms:
Product Documents:
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| 1G |
$65.00
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| 5G |
$208.00
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| Product Number | B1768 |
| Purity / Analysis Method | >94.0%(GC) |
| Molecular Formula / Molecular Weight | C__1__0H__2__2O__2Si__2 = 230.45 |
| Physical State (20 deg.C) | Liquid |
| Storage Temperature | Room Temperature (Recommended in a cool and dark place, <15°C) |
| Store Under Inert Gas | Store under inert gas |
| Condition to Avoid | Moisture Sensitive |
| CAS RN | 17082-61-0 |
| Reaxys Registry Number | 1367530 |
| PubChem Substance ID | 87564663 |
| MDL Number | MFCD00010798 |
Specifications
| Appearance | Colorless to Light yellow clear liquid |
| Purity(GC) | min. 94.0 % |
Properties (reference)
| Boiling Point | 59 °C/2 mmHg |
| Flash point | 61 °C |
| Specific Gravity (20/20) | 0.90 |
| Refractive Index | 1.43 |
GHS
| Pictogram |
|
| Signal Word | Warning |
| Hazard Statements | H315 : Causes skin irritation. H319 : Causes serious eye irritation. H227 : Combustible liquid. |
| Precautionary Statements | P501 : Dispose of contents/ container to an approved waste disposal plant. P210 : Keep away from heat/sparks/open flames/hot surfaces. No smoking. P264 : Wash skin thoroughly after handling. P280 : Wear protective gloves/ eye protection/ face protection. P302 + P352 : IF ON SKIN: Wash with plenty of water. P370 + P378 : In case of fire: Use dry sand, dry chemical or alcohol-resistant foam to extinguish. P337 + P313 : If eye irritation persists: Get medical advice/ attention. P305 + P351 + P338 : IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. P362 + P364 : Take off contaminated clothing and wash it before reuse. P332 + P313 : If skin irritation occurs: Get medical advice/ attention. P403 + P235 : Store in a well-ventilated place. Keep cool. |
Related Laws:
Transport Information:
| H.S.code* | 2931.90-000 |
Application
Disilyloxycyclobutene
References
Aldol-type reactions a) A novel ring-opening reaction
E. Nakamura, K. Hashimoto, I. Kuwajima, J. Org. Chem. 1977, 42, 4166.
b) Geminal acylation via pinacol rearrangement
E. Nakamura, I. Kuwajima, J. Am. Chem. Soc. 1977, 99, 961.
c) Ring expansion and cleavage of succinoin derivatives
J. Shimada, K. Hashimoto, B. H. Kim, E. Nakamura, I. Kuwajima, J. Am. Chem. Soc. 1984, 106, 1759.
Photocycloaddition reactions a) Diterpene total synthesis
L. V. Hijfte, M. Vandewalle, Synth. Commun. 1984, 14, 1149.
b) The total synthesis of 1-oxygenated eudesmanolides
L. V. Hijfte, M. Vandewalle, Tetrahedron 1984, 40, 4371.
Precursor to 1,2-Cyclobutanedione and 2-Hydroxycyclobutanone
J. J. Bloomfield, J. M. Nelke, ibid. 1977, 57, 1.
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