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Published TCIMAIL newest issue No.197
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CAS RN: 20082-71-7 | Product Number: P0854
Pentafluorophenyldimethylchlorosilane [Pentafluorophenyldimethylsilylating Agent]
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![Pentafluorophenyldimethylchlorosilane [Pentafluorophenyldimethylsilylating Agent]](/_ui/responsive/theme-tci/images/missing_product_zoom.jpg "Pentafluorophenyldimethylchlorosilane [Pentafluorophenyldimethylsilylating Agent]")
Purity: >95.0%(GC)
Synonyms:
- Dimethylpentafluorophenylchlorosilane
- Flophemesyl Chloride
Product Documents:
| Size | Unit Price | Belgium | Japan* | Quantity |
|---|---|---|---|---|
| 1ML |
82,00 €
|
1 | 14 |
|
| 5ML |
383,00 €
|
Contact Us | 8 |
|
*Stock available in Belgium will be delivered in 1 to 3 days
*Stock available in Japan will be delivered in 1 to 2 weeks (excludes regulated items and dry ice shipments).
| Product Number | P0854 |
| Purity / Analysis Method | >95.0%(GC) |
| Molecular Formula / Molecular Weight | C__8H__6ClF__5Si = 260.66 |
| Physical State (20 deg.C) | Liquid |
| Storage Temperature | Room Temperature (Recommended in a cool and dark place, <15°C) |
| Store Under Inert Gas | Store under inert gas |
| Condition to Avoid | Moisture Sensitive |
| CAS RN | 20082-71-7 |
| Reaxys Registry Number | 2858407 |
| PubChem Substance ID | 87574981 |
| SDBS (AIST Spectral DB) | 23275 |
| MDL Number | MFCD00000500 |
Specifications
| Appearance | Colorless to Almost colorless clear liquid |
| Purity(GC) | min. 95.0 % |
| NMR | confirm to structure |
Properties (reference)
| Boiling Point | 47 °C/1 mmHg |
| Flash point | 75 °C |
| Specific Gravity (20/20) | 1.41 |
| Refractive Index | 1.45 |
GHS
| Pictogram |
|
| Signal Word | Danger |
| Hazard Statements | H314 : Causes severe skin burns and eye damage. H290 : May be corrosive to metals. |
| Precautionary Statements | P280 : Wear protective gloves/ protective clothing/ eye protection/ face protection/ hearing protection. P390 : Absorb spillage to prevent material damage. P303 + P361 + P353 : IF ON SKIN (or hair): Take off immediately all contaminated clothing. Rinse skin with water. P301 + P330 + P331 : IF SWALLOWED: Rinse mouth. Do NOT induce vomiting. P304 + P340 + P310 : IF INHALED: Remove person to fresh air and keep comfortable for breathing. Immediately call a POISON CENTER/doctor. P305 + P351 + P338 + P310 : IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. Immediately call a POISON CENTER/doctor. |
Related Laws:
| EC Number | 243-506-9 |
Transport Information:
| UN Number | UN2985 |
| Class | 3 / 8 |
| Packing Group | II |
| HS Number | 2931900090 |
Application
Silylating Reagent for GC-ECD
Experimental procedure:
The substrate (primary alcohol) is dissolved in pyridine and 1:1 mixture of pentafluorophenyldimethylsilyldiethylamine and pentafluorophenyldimethylchlorosilane is subsequently added. This mixture can be directly used for GC-ECD analysis. In the case of tertiary alcohols, the derivatization is completed by reacting for 10 min at 25 °C.
The substrate (primary alcohol) is dissolved in pyridine and 1:1 mixture of pentafluorophenyldimethylsilyldiethylamine and pentafluorophenyldimethylchlorosilane is subsequently added. This mixture can be directly used for GC-ECD analysis. In the case of tertiary alcohols, the derivatization is completed by reacting for 10 min at 25 °C.
References
- Detection of alcohols at the femtogram level as pentafluorophenyldimethylsilyl ethers
PubMed Literature
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