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CAS RN: 86393-33-1 | Product Number: C2293
7-Chloro-1-cyclopropyl-6-fluoro-1,4-dihydro-4-oxoquinoline-3-carboxylic Acid
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Purity: >98.0%(T)(HPLC)
Synonyms:
- Fluoroquinolonic Acid
Product Documents:
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|---|---|---|---|---|---|
| 5G |
$18.00
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6 | ≥60 | Contact Us | |
| 25G |
$53.00
|
1 | 25 | Contact Us |
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| Product Number | C2293 |
| Purity / Analysis Method | >98.0%(T)(HPLC) |
| Molecular Formula / Molecular Weight | C__1__3H__9ClFO__3N = 281.67 |
| Physical State (20 deg.C) | Solid |
| Storage Temperature | Room Temperature (Recommended in a cool and dark place, <15°C) |
| CAS RN | 86393-33-1 |
| Reaxys Registry Number | 4515704 |
| PubChem Substance ID | 87560826 |
| MDL Number | MFCD00792458 |
Specifications
| Appearance | White to Light yellow powder to crystal |
| Purity(HPLC) | min. 98.0 area% |
| Purity(Neutralization titration) | min. 98.0 % |
Properties (reference)
| Melting Point | 244 °C |
GHS
| Pictogram |
|
| Signal Word | Warning |
| Hazard Statements | H302 : Harmful if swallowed. H412 : Harmful to aquatic life with long lasting effects. |
| Precautionary Statements | P501 : Dispose of contents/ container to an approved waste disposal plant. P273 : Avoid release to the environment. P270 : Do not eat, drink or smoke when using this product. P264 : Wash skin thoroughly after handling. P301 + P312 + P330 : IF SWALLOWED: Call a POISON CENTER/doctor if you feel unwell. Rinse mouth. |
Related Laws:
| RTECS# | VB1993795 |
Transport Information:
| H.S.code* | 2933.49-000 |
Application
Amination with morpholine derivatives under microwave irradiation
Reference
Application
Synthesis and metabolic evaluation of azaspirocyclic fluoroquinolones
Typical procedure: KOtBu (191 mg) is dissolve in DMSO (20 mL), azetidinium oxalate (164 mg) is added and the mixture is stirred at rt for 10 min. Then, 7-chloro-1-cyclopropyl-6-fluoro-1,4-dihydro-4-oxoquinoline-3-carboxylic acid (200 mg) is added, and the yellow mixture is heated to 130 °C and stirred for 5.5 h. Then it is cooled to rt and poured into H2O (75 mL). The precipitate is filtered and dried overnight upon standing. The crude product is purified by suspending in hot CHCl3, and cooling the mixture to rt, when it is filtered. The residue is dried in vacuo to give the pure desired product (166 mg, 68 %).
References
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