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CAS RN: 1648825-53-9 | Product Number: P2420
PhenoFluor™ Mix
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Purity:
Synonyms:
- 2-Chloro-1,3-bis(2,6-diisopropylphenyl)-1H-imidazolium Chloride - Cesium Fluoride
Product Documents:
| Size | Unit Price | Philadelphia, PA | Portland, OR | Japan* | Quantity |
|---|---|---|---|---|---|
| 1G |
$292.00
|
1 | 1 | 11 |
|
| 5G |
$876.00
|
3 | 1 | 9 |
|
* Items in stock locally ship in 1-2 business days. Items from Japan stock are able to ship from a US warehouse within 2 weeks. Please contact TCI for lead times on items not in stock. Excludes regulated items and items that ship on ice.
* To send your quote request for bulk quantities, please click on the "Request Quote" button. Please note that we cannot offer bulk quantities for some products.
*TCI frequently reviews storage conditions to optimize them. Please note that the latest information on the storage temperature for the products is described on our website.
Supplemental Product Information:
PhenoFluor™ is a trademark of SciFluor Life Sciences, Inc.
| Product Number | P2420 |
| Molecular Formula / Molecular Weight | C__2__7H__3__6Cl__2N__2·xCsF |
| Physical State (20 deg.C) | Solid |
| Storage Temperature | Room Temperature (Recommended in a cool and dark place, <15°C) |
| Store Under Inert Gas | Store under inert gas |
| Condition to Avoid | Moisture Sensitive |
| Packaging and Container | 1G-Glass Bottle with Plastic Insert (View image) |
| CAS RN | 1648825-53-9 |
| PubChem Substance ID | 354334397 |
Specifications
| Appearance | White to Almost white powder to crystal |
| Assay | 30.0 to 32.0w% [as 2-Chloro-1,3-bis(2,6-diisopropylphenyl)-1H-imidazolium Chloride] |
| NMR | confirm to structure |
Properties (reference)
| Melting Point | 229 °C |
GHS
| Pictogram |
|
| Signal Word | Danger |
| Hazard Statements | H301 + H311 + H331 : Toxic if swallowed, in contact with skin or if inhaled. H314 : Causes severe skin burns and eye damage. |
| Precautionary Statements | P501 : Dispose of contents/ container to an approved waste disposal plant. P260 : Do not breathe dusts or mists. P270 : Do not eat, drink or smoke when using this product. P271 : Use only outdoors or in a well-ventilated area. P264 : Wash skin thoroughly after handling. P280 : Wear protective gloves/ protective clothing/ eye protection/ face protection. P303 + P361 + P353 : IF ON SKIN (or hair): Take off immediately all contaminated clothing. Rinse skin with water/shower. P301 + P330 + P331 : IF SWALLOWED: Rinse mouth. Do NOT induce vomiting. P362 : Take off contaminated clothing and wash before reuse. P301 + P310 + P330 : IF SWALLOWED: Immediately call a POISON CENTER/doctor. Rinse mouth. P304 + P340 + P310 : IF INHALED: Remove person to fresh air and keep comfortable for breathing. Immediately call a POISON CENTER/doctor. P305 + P351 + P338 + P310 : IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. Immediately call a POISON CENTER/doctor. P403 + P233 : Store in a well-ventilated place. Keep container tightly closed. P405 : Store locked up. |
Related Laws:
Transport Information:
| UN Number (DOT-AIR) | UN2923 |
| Class (DOT-AIR) | 8/6.1 |
| Packing Group (TCI-A) | III |
| HS Number | 2933.29.9000 |
Application
PhenoFluorTM Mix: Stable Agent for Deoxyfluorination
Experimental procedure: A mixture of 4-(methylsufonyl)phenol (88.8 mg, 0.500 mmol) and PhenoFluorTM Mix (1.10 g) in toluene (5.0 mL) is stirred at 23 °C for 30 min, then at 110 °C for 24 h. Purification by flash silica gel column chromatography (hexanes:EtOAc = 9:1 - 7:3) affords the desired compound as a colorless solid (86.4 mg, 99% yield).
References
- PhenoFluorMix: Practical Chemoselective Deoxyfluorination of Phenols
Articles/Brochures
TCIMAIL
[Product Highlights] PhenoFluor™ Mix and AlkylFluor™: Stable Reagents for DeoxyfluorinationsProduct Documents (Note: Some products will not have analytical charts available.)
Safety Data Sheet (SDS)
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Specifications
C of A & Other Certificates
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Analytical Charts
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