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CAS RN: 1440939-88-7 | Product Number: C2728
N-[(9S)-8α-Cinchonan-9-yl]quinoline-8-sulfonamide
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![N-[(9S)-8α-Cinchonan-9-yl]quinoline-8-sulfonamide](/_ui/responsive/theme-tci/images/missing_product_zoom.jpg "N-[(9S)-8α-Cinchonan-9-yl]quinoline-8-sulfonamide")
Purity: >98.0%(HPLC)
Synonyms:
- (S)-N-8-Quinolinesulfonyl-(quinolin-4-yl)(8-vinylquinuclidin-2-yl)methanamine
Product Documents:
| Size | Unit Price | Philadelphia, PA | Portland, OR | Japan* | Quantity |
|---|---|---|---|---|---|
| 100MG |
$194.00
|
Contact Us | 2 | 2 |
|
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| Product Number | C2728 |
| Purity / Analysis Method | >98.0%(HPLC) |
| Molecular Formula / Molecular Weight | C__2__8H__2__8N__4O__2S = 484.62 |
| Physical State (20 deg.C) | Solid |
| Storage Temperature | Room Temperature (Recommended in a cool and dark place, <15°C) |
| Packaging and Container | 100MG-Glass Bottle with Plastic Insert (View image) |
| CAS RN | 1440939-88-7 |
| Reaxys Registry Number | 22760573 |
| PubChem Substance ID | 253660147 |
Specifications
| Appearance | White to Yellow powder to crystal |
| Purity(HPLC) | min. 98.0 area% |
| Elemental analysis(Nitrogen) | 10.80 to 12.00 % |
| Specific rotation | +108 to +114 deg(C=1, CHCl3) |
| NMR | confirm to structure |
Properties (reference)
| Melting Point | 260 °C |
GHS
Related Laws:
Transport Information:
| HS Number | 2935.90.9500 |
Application
Heteroarenesulfonyl Cinchona Alkaloid Amine Catalyst
Typical Procedure (Entry 1):
To a solution of ketimine (0.038 mmol, 10.0 mg) and 1 (0.008 mmol, 3.9 mg) in CPME (0.5 mL), malonic acid half thioester (0.084 mmol, 16.4 mg) is added and stirred for 48 h. After removal of solvent, the residue is purified by silica gel column chromatography (hexane : AcOEt = 80 : 20) to afford the (S)-product (14.3 mg, Y. 91%) as a white solid.
To a solution of ketimine (0.038 mmol, 10.0 mg) and 1 (0.008 mmol, 3.9 mg) in CPME (0.5 mL), malonic acid half thioester (0.084 mmol, 16.4 mg) is added and stirred for 48 h. After removal of solvent, the residue is purified by silica gel column chromatography (hexane : AcOEt = 80 : 20) to afford the (S)-product (14.3 mg, Y. 91%) as a white solid.
References
- 1)Heteroarenesulfonyl cinchona alkaloid amine catalyst and method for the preparation of β-aminocarbonyl compound thereby
- S. Nakamura, N. Shibata, N. Hara, Nagoya Institute of Technology, Jpn. Kokai Tokkyo Koho 2013 112673, 2013.
- 2)Enantioselective synthesis of AG-041R by using N-heteroarenesulfonyl cinchona alkaloid amides as organocatalysts
PubMed Literature
Articles/Brochures
TCIMAIL
[TCIMAIL No.161] Heteroarenesulfonyl Cinchona Alkaloid Amine Catalyst[Research Articles] Heteroarenesulfonyl Cinchona Alkaloid Amine Catalyst
Product Documents (Note: Some products will not have analytical charts available.)
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