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CAS RN: 37091-73-9 | Product Number: C1408
2-Chloro-1,3-dimethylimidazolinium Chloride
Purity: >98.0%(HPLC)
Synonyms:
- DMC
Product Documents:
Size | Unit Price | Saitama (Kawaguchi) | Hyogo (Amagasaki) | Stock in other WH | Shipping Information |
---|---|---|---|---|---|
5G |
¥5,800
|
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25G |
¥18,500
|
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* The displayed price is the unit price and does not include consumption tax. The unit prices displayed are the latest and are subject to change without notice.
* To send your quote request for bulk quantities, please click on the "Request Bulk Quote" button. Please note that we cannot offer bulk quantities for some products.
*TCI frequently reviews storage conditions to optimize them. Please note that the latest information on the storage temperature for the products is described on our website.
Product Number | C1408 |
Purity / Analysis Method | >98.0%(HPLC) |
Molecular Formula / Molecular Weight | C__5H__1__0Cl__2N__2 = 169.05 |
Physical State (20 deg.C) | Solid |
Storage Temperature | Room Temperature (Recommended in a cool and dark place, <15°C) |
Store Under Inert Gas | Store under inert gas |
Condition to Avoid | Hygroscopic |
CAS RN | 37091-73-9 |
Reaxys Registry Number | 4014485 |
PubChem Substance ID | 87566416 |
SDBS (AIST Spectral DB) | 19638 |
MDL Number | MFCD00137463 |
Specifications
Appearance | White to Light yellow to Light orange powder to crystal |
Purity(HPLC) | min. 98.0 area% |
Purity(with Total Nitrogen) | min. 97.0 % |
Properties (reference)
GHS
Pictogram | |
Signal Word | Warning |
Hazard Statements | H315 : Causes skin irritation. H319 : Causes serious eye irritation. |
Precautionary Statements | P264 : Wash skin thoroughly after handling. P280 : Wear protective gloves/ eye protection/ face protection. P302 + P352 : IF ON SKIN: Wash with plenty of water. P337 + P313 : If eye irritation persists: Get medical advice/ attention. P305 + P351 + P338 : IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. P362 + P364 : Take off contaminated clothing and wash it before reuse. P332 + P313 : If skin irritation occurs: Get medical advice/ attention. |
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Application
Condensing Agent
Experimental procedure1): To a solution of 3-phenylpropionic Acid (1.0 eq.), tert-butyl alcohol (1.0 eq.), and DMC (1.0 eq.) in dichloromethane is added dropwise pyridine (2.0 eq.) at room temperature. The mixture is stirred for 20 h at room temperature, poured into water, and extracted with dichloromethane. The organic solution is successively washed with 5% HCl, aqueous saturated NaHCO3, and water. It is dried (MgSO4) and evaporated to dryness. The residue is purified by silica gel column chromatography to give 1 in 91% yield.
References
- 1) 2-Chloro-1,3-dimethylimidazolinium Chloride. 1. A Powerful Dehydrating Equivalent to DCC
- 2) 2-Chloro-1,3-dimethylimidazolinium Chloride. 2. Its Application to the Construction of Heterocycles through Dehydration Reactions
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