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CAS RN: 50296-37-2 | Product Number: B3838
Bromotris(dimethylamino)phosphonium Hexafluorophosphate
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Purity: >98.0%(T)(HPLC)
Synonyms:
- BroP
Product Documents:
| Size | Unit Price | Saitama (Kawaguchi) | Hyogo (Amagasaki) | Stock in other WH |
Shipping Information
|
|---|---|---|---|---|---|
| 1G |
¥4,000
|
4 | 7 | Contact Us | |
| 5G |
¥13,700
|
6 | 13 | 30 |
* Available Stock: Prompt shipment (for products) in Saitama/Hyogo warehouse. Stock In Other WH: Shipment in about 2-3 Business Days from Saitama warehouse. Please contact us
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*TCI frequently reviews storage conditions to optimize them. Please note that the latest information on the storage temperature for the products is described on our website.
* The displayed price is the unit price and does not include consumption tax. The unit prices displayed are the latest and are subject to change without notice.
* To send your quote request for bulk quantities, please click on the "Request Bulk Quote" button. Please note that we cannot offer bulk quantities for some products.
*TCI frequently reviews storage conditions to optimize them. Please note that the latest information on the storage temperature for the products is described on our website.
| Product Number | B3838 |
Purity / Analysis Method 
|
>98.0%(T)(HPLC) |
| Molecular Formula / Molecular Weight | C__6H__1__8BrF__6N__3P__2 = 388.07 |
| Physical State (20 deg.C) | Solid |
| Storage Temperature
|
Room Temperature (Recommended in a cool and dark place, <15°C) |
| Packaging and Container
|
1G-Glass Bottle with Plastic Insert (View image) |
| CAS RN | 50296-37-2 |
| Reaxys Registry Number | 14221932 |
| PubChem Substance ID | 160870946 |
| MDL Number | MFCD00191864 |
Specifications
| Appearance | White to Almost white powder to crystal |
| Purity(HPLC) | min. 98.0 area% |
| Purity(Argentometric Titration) | min. 98.0 % |
Properties (reference)
GHS
| Pictogram |
|
| Signal Word | Danger |
| Hazard Statements | H314 : Causes severe skin burns and eye damage. |
| Precautionary Statements | P501 : Dispose of contents/ container to an approved waste disposal plant. P260 : Do not breathe dust. P264 : Wash skin thoroughly after handling. P280 : Wear protective gloves/ protective clothing/ eye protection/ face protection. P303 + P361 + P353 : IF ON SKIN (or hair): Take off immediately all contaminated clothing. Rinse skin with water. P301 + P330 + P331 : IF SWALLOWED: Rinse mouth. Do NOT induce vomiting. P363 : Wash contaminated clothing before reuse. P304 + P340 + P310 : IF INHALED: Remove person to fresh air and keep comfortable for breathing. Immediately call a POISON CENTER/doctor. P305 + P351 + P338 + P310 : IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. Immediately call a POISON CENTER/doctor. P405 : Store locked up. |
Related Laws:
Transport Information:
| UN Number | UN1759 |
| Class | 8 |
| Packing Group | II |
Application
A Condensing Agent
Experimental procedure2): A solution of 1 (80 mg, 0.189 mmol, 1.0 eq.) in acetonitrile (1.5 mL) and diethylamine (1.5 mL) is stirred at room temperature under N2 for 30 min and then concentrated. The residue is concentrated twice more from acetonitrile and then suspended in CH2Cl2 (3 mL) under N2. To this is added 2 (77 mg, 0.199 mmol, 1.15 eq.), DIPA (82 μL, 0.473 mmol, 2.5 eq.), and BroP (77 mg, 0.199 mmol, 1.05 eq.). The flask is flushed with N2, stoppered, and left to stir at room temperature overnight. The mixture is concentrated and the residue applied to a flash column in a minimum volume of CH2Cl2. The column is eluted with 3:1 EtOAc - hexanes to afford 3 (106 mg, 98% yield).
References
- 1)Brop: A new reagent for coupling N-methylated amino acids
- 2)The Impact of Pyrrolidine Hydroxylation on the Conformation of Proline-Containing Peptides
PubMed Literature
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