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CAS RN: 14548-46-0 | Product Number: B0306
4-Benzoylpyridine
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Purity: >99.0%(T)
Synonyms:
- Phenyl 4-Pyridyl Ketone
Product Documents:
| Size | Unit Price | Saitama (Kawaguchi) | Hyogo (Amagasaki) | Stock in other WH |
Shipping Information
|
|---|---|---|---|---|---|
| 25G |
¥4,900
|
17 | 5 | 24 |
* Available Stock: Prompt shipment (for products) in Saitama/Hyogo warehouse. Stock In Other WH: Shipment in about 2-3 Business Days from Saitama warehouse. Please contact us
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* The displayed price is the unit price and does not include consumption tax. The unit prices displayed are the latest and are subject to change without notice.
* To send your quote request for bulk quantities, please click on the "Request Bulk Quote" button. Please note that we cannot offer bulk quantities for some products.
*TCI frequently reviews storage conditions to optimize them. Please note that the latest information on the storage temperature for the products is described on our website.
| Product Number | B0306 |
| Purity / Analysis Method | >99.0%(T) |
| Molecular Formula / Molecular Weight | C__1__2H__9NO = 183.21 |
| Physical State (20 deg.C) | Solid |
| Storage Temperature | Room Temperature (Recommended in a cool and dark place, <15°C) |
| CAS RN | 14548-46-0 |
| Reaxys Registry Number | 3864 |
| PubChem Substance ID | 87563396 |
| SDBS (AIST Spectral DB) | 1769 |
| MDL Number | MFCD00006430 |
Specifications
| Appearance | White to Orange to Green powder to crystal |
| Purity(GC) | min. 98.0 % |
| Purity(Nonaqueous Titration) | min. 99.0 % |
| Melting point | 70.0 to 73.0 °C |
| Solubility in Methanol | almost transparency |
| NMR | confirm to structure |
Properties (reference)
| Melting Point | 72 °C |
| Boiling Point | 130 °C/1 mmHg |
| Solubility (soluble in) | Methanol |
GHS
| Pictogram |
|
| Signal Word | Warning |
| Hazard Statements | H315 : Causes skin irritation. H319 : Causes serious eye irritation. |
| Precautionary Statements | P264 : Wash skin thoroughly after handling. P280 : Wear protective gloves/ eye protection/ face protection. P302 + P352 : IF ON SKIN: Wash with plenty of water. P337 + P313 : If eye irritation persists: Get medical advice/ attention. P305 + P351 + P338 : IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. P362 + P364 : Take off contaminated clothing and wash it before reuse. P332 + P313 : If skin irritation occurs: Get medical advice/ attention. |
Related Laws:
| RTECS# | OB6402000 |
Transport Information:
Application
Oxidant for Photo-oxidation of Alcohols
Experimental procedure: An acetone solution (5 mL) of cyclododecanol (92.2 mg, 0.5 mmol) and 4-benzoylpyridine (109.9 mg, 0.6 mmol) is placed in a test tube under Ar atmosphere. The test tube is placed at ca. 5 cm distance from a UV-lamp and is irradiated using a 100 W medium-pressure mercury lamp at room temperature for 48 h. After consumption of the alcohol, the solution is evaporated to remove volatile materials. The residue is purified by silica gel column chromatography (hexane:AcOEt = 100:1 - 10:1) to afford cyclododecanone in 78% yield (70.7 mg).
References
- Photoinduced Oxidation of Secondary Alcohols Using 4-Benzoylpyridine as an Oxidant
PubMed Literature
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