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CAS RN: 174501-64-5 | Product Number: B2320
1-Butyl-3-methylimidazolium Hexafluorophosphate
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Purity: >98.0%(HPLC)(N)
Synonyms:
- BMIMPF6
Product Documents:
| Size | Unit Price | Belgium | Japan* | Quantity |
|---|---|---|---|---|
| 5G |
24,00 €
|
2 | 25 |
|
| 25G |
77,00 €
|
7 | ≥100 |
|
*Stock available in Belgium will be delivered in 1 to 3 days
*Stock available in Japan will be delivered in 1 to 2 weeks (excludes regulated items and dry ice shipments).
| Product Number | B2320 |
| Purity / Analysis Method | >98.0%(HPLC)(N) |
| Molecular Formula / Molecular Weight | C__8H__1__5F__6N__2P = 284.19 |
| Physical State (20 deg.C) | Liquid |
| Storage Temperature | Room Temperature (Recommended in a cool and dark place, <15°C) |
| Store Under Inert Gas | Store under inert gas |
| Condition to Avoid | Hygroscopic |
| CAS RN | 174501-64-5 |
| Reaxys Registry Number | 8026031 |
| PubChem Substance ID | 87565152 |
| Merck Index (14) | 1581 |
| MDL Number | MFCD03093295 |
Specifications
| Purity(HPLC) | min. 98.0 area% |
| Purity(with Total Nitrogen) | min. 98.0 % |
Properties (reference)
| Specific Gravity (20/20) | 1.37 |
| Refractive Index | 1.41 |
| Solubility in water | Completely miscible |
| Solubility (insoluble in) | Toluene |
GHS
| Pictogram |
|
| Signal Word | Warning |
| Hazard Statements | H315 : Causes skin irritation. H319 : Causes serious eye irritation. |
| Precautionary Statements | P264 : Wash skin thoroughly after handling. P280 : Wear protective gloves/ eye protection/ face protection. P302 + P352 : IF ON SKIN: Wash with plenty of water. P337 + P313 : If eye irritation persists: Get medical advice/ attention. P362 + P364 : Take off contaminated clothing and wash it before reuse. P332 + P313 : If skin irritation occurs: Get medical advice/ attention. |
Related Laws:
Transport Information:
| HS Number | 2933299090 |
Application
Hydrotrope research
Hydrotropes are small molecules able to enhance the solubility of hydrophobic substances in aqueous media. Their water-solubility can significantly enhance the solubility of organic solutes such as esters, alcohols, aldehydes, ketones, hydrocarbons, and fats.1) 1-Butyl-3-methylimidazolium hexafluorophosphate has been reported to enhance the solubility of danazol and ibuprofen (I0415).2,3)
(The product is for research purpose only.)
(The product is for research purpose only.)
References
- 1) Action of hydrotropes and alkyl-hydrotropes
- 2) Ionic liquids provide unique opportunities for oral drug delivery: structure optimization and in vivo evidence of utility
- 3) Solubilities of Pharmaceutical Compounds in Ionic Liquids
Application
Synthesis of quinolines via Friedländer annulation in an ionic liquid
Typical procedure: A mixture of 2-aminobenzophenone (197 mg), ethyl acetoacetate (169 mg) and CAN (27 mg) in BMIMPF6 (2 mL) ionic liquid is stirred at 60 °C for 30 min. Subsequently, the reaction mixture is extracted with EtOAc and dried over MgSO4. After filtration, the mixture is concentrated under reduced pressure and the residue is purified by chromatography on silica gel (eluent: hexane/EtOAc = 3/1) to give the desired quinoline (268 mg, 92 %). The remaining ionic liquid is dried at 80 °C under reduced pressure and reused in subsequent runs.
References
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