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CAS RN: 1443438-29-6 | Product Number: P2298
(R)-1-(3-Pyridylthiocarbamoyl)pyrrolidine-2-carboxylic Acid
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Purity: >98.0%(T)(HPLC)
Synonyms:
- (R)-PyT-C
Product Documents:
| Size | Unit Price | Belgium | Japan* | Quantity |
|---|---|---|---|---|
| 100MG |
€133.00
|
1 | 29 |
|
*Stock available in Belgium will be delivered in 1 to 3 days
*Stock available in Japan will be delivered in 1 to 2 weeks (excludes regulated items and dry ice shipments).
| Product Number | P2298 |
| Purity / Analysis Method | >98.0%(T)(HPLC) |
| Molecular Formula / Molecular Weight | C__1__1H__1__3N__3O__2S = 251.30 |
| Physical State (20 deg.C) | Solid |
| Storage Temperature | Room Temperature (Recommended in a cool and dark place, <15°C) |
| CAS RN | 1443438-29-6 |
| PubChem Substance ID | 354333476 |
Specifications
| Appearance | White to Almost white powder to crystal |
| Purity(HPLC) | min. 98.0 area% |
| Purity(Neutralization titration) | min. 98.0 % |
| Specific rotation [a]20/D | +58.0 to +62.0 deg(C=1, 6mol/l HCl) |
| NMR | confirm to structure |
Properties (reference)
| Melting Point | 192 °C(dec.) |
| Specific Rotation | 60° (C=1,6mol/L HCl) |
GHS
| Pictogram |
|
| Signal Word | Warning |
| Hazard Statements | H315 : Causes skin irritation. H319 : Causes serious eye irritation. |
| Precautionary Statements | P264 : Wash skin thoroughly after handling. P280 : Wear protective gloves/ eye protection/ face protection. P302 + P352 : IF ON SKIN: Wash with plenty of water. P337 + P313 : If eye irritation persists: Get medical advice/ attention. P362 + P364 : Take off contaminated clothing and wash it before reuse. P332 + P313 : If skin irritation occurs: Get medical advice/ attention. |
Related Laws:
Transport Information:
| HS Number | 2933399990 |
Application
Chiral Derivatization Reagent Possessing a Pyridylthiourea Structure
Typical Procedure:
A 10 mM 1 in acetonitrile (20 µL) is reacted at 60 °C for 60 min with chiral amines (10 µM) in the presence of 10 mM triphenylphosphine in acetonitrile (20 µL) and 10 mM 2,2'-dipyridyl disulfide in acetonitrile (20 µL). After removal of the solvent under a gentle nitrogen stream, the residues are re-dissolved in the initial mobile phase, and then an aliquot (2 µL) is subjected to UHPLC-ESI-MS/MS. The separations of the pair of diastereomers for chiral amines are performed by isocratic elution using water/acetonitrile containing 0.1% formic acid. The SRM chromatograms of each pair of diastereomers are obtained from the monitoring ion of m/z 137.0, derived from the MS transition of corresponding protonated-molecular ion, [M+H]+.
A 10 mM 1 in acetonitrile (20 µL) is reacted at 60 °C for 60 min with chiral amines (10 µM) in the presence of 10 mM triphenylphosphine in acetonitrile (20 µL) and 10 mM 2,2'-dipyridyl disulfide in acetonitrile (20 µL). After removal of the solvent under a gentle nitrogen stream, the residues are re-dissolved in the initial mobile phase, and then an aliquot (2 µL) is subjected to UHPLC-ESI-MS/MS. The separations of the pair of diastereomers for chiral amines are performed by isocratic elution using water/acetonitrile containing 0.1% formic acid. The SRM chromatograms of each pair of diastereomers are obtained from the monitoring ion of m/z 137.0, derived from the MS transition of corresponding protonated-molecular ion, [M+H]+.
References
PubMed Literature
Articles/Brochures
TCIMAIL
[TCIMAIL No.169] Chiral Derivatization Reagent Possessing a Pyridylthiourea Structure[Product Highlights] Chiral Derivatization Reagent Possessing a Pyridylthiourea Structure
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