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Published TCIMAIL newest issue No.197
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CAS RN: 73482-96-9 | Product Number: R0161
Rhodium(II) Octanoate Dimer
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Purity:
Synonyms:
- Tetrakis(octanoato)dirhodium(II)
Product Documents:
| Size | Unit Price | Belgium | Japan* | Quantity |
|---|---|---|---|---|
| 200MG |
€121.00
|
1 | 4 |
|
| 1G |
€450.00
|
2 | ≥40 |
|
*Stock available in Belgium will be delivered in 1 to 3 days
*Stock available in Japan will be delivered in 1 to 2 weeks (excludes regulated items and dry ice shipments).
| Product Number | R0161 |
| Molecular Formula / Molecular Weight | C__3__2H__6__0O__8Rh__2 = 778.64 |
| Physical State (20 deg.C) | Solid |
| Storage Temperature | Room Temperature (Recommended in a cool and dark place, <15°C) |
| CAS RN | 73482-96-9 |
| Reaxys Registry Number | 14206645 |
| PubChem Substance ID | 253662547 |
| MDL Number | MFCD00064724 |
Specifications
| Appearance | Green to Dark green powder to crystal |
| Elemental analysis(Carbon) | 47.00 to 52.00 % |
Properties (reference)
GHS
Related Laws:
Transport Information:
| HS Number | 2843909000 |
Application
An Intramolecular C-H Amination of Aryl Azides
Experimental procedure: to a mixture of 1 (0.056 g, 0.246 mmol), Rh2(O2CC7H15)4 (0.012 mmol) and 4A molecular sieves (0.056 g) is added 1,2-dichloroethane (0.2 mL). The resulting mixture is heated to 60 °C. After 16 h, the reaction mixture is cooled to room temperature, and the heterogenous mixture is filtered through SiO2. The filtrate is concentrated in vacuo. Purification by MPLC (EtOAc:hexanes = 0:100 – 5:95) affords 2 (0.034 g, 69% yield) as a white solid.
References
- Dirhodium(II)-Catalyzed Intramolecular C-H Amination of Aryl Azides
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