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CAS RN: 156-62-7 | Product Number: C0006
Calcium Cyanamide
Purity:
Synonyms:
Product Documents:
Size | Unit Price | Belgium | Japan* | Quantity |
---|---|---|---|---|
25G |
€16.00
|
Contact Us | 9 |
|
500G |
€59.00
|
1 | 1 |
|
*Stock available in Belgium will be delivered in 1 to 3 days
*Stock available in Japan will be delivered in 1 to 2 weeks (excludes regulated items and dry ice shipments).
Product Number | C0006 |
Molecular Formula / Molecular Weight | CCaN__2 = 80.10 |
Physical State (20 deg.C) | Solid |
Storage Temperature | Room Temperature (Recommended in a cool and dark place, <15°C) |
Store Under Inert Gas | Store under inert gas |
Condition to Avoid | Moisture Sensitive |
CAS RN | 156-62-7 |
Reaxys Registry Number | 3912122 |
PubChem Substance ID | 87565218 |
SDBS (AIST Spectral DB) | 10626 |
Merck Index (14) | 1662 |
MDL Number | MFCD00064894 |
Specifications
Appearance | Light gray to Brown to Black powder to crystal |
Nitorogen of cyanamide | min. 19.5 % |
Properties (reference)
GHS
Pictogram | |
Signal Word | Danger |
Hazard Statements | H302 : Harmful if swallowed. H315 : Causes skin irritation. H318 : Causes serious eye damage. H371 : May cause damage to organs. H335 : May cause respiratory irritation. H411 : Toxic to aquatic life with long lasting effects. H261 : In contact with water releases flammable gases. |
Precautionary Statements | P273 : Avoid release to the environment. P260 : Do not breathe dust. P231 + P232 : Handle and store contents under inert gas. Protect from moisture. P280 : Wear protective gloves/ protective clothing/ eye protection/ face protection/ hearing protection. P370 + P378 : In case of fire: Use dry sand, dry chemical or alcohol-resistant foam to extinguish. P391 : Collect spillage. P305 + P351 + P338 + P310 : IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. Immediately call a POISON CENTER/doctor. |
Related Laws:
EC Number | 205-861-8 |
RTECS# | GS6000000 |
Transport Information:
UN Number | UN1403 |
Class | 4.3 |
Packing Group | III |
HS Number | 3102900090 |
Application
Preparation of Cyanamide
Typical Procedure:Glacial acetic acid 57 g (54 mL, 0.75 mol) and water 135 mL are placed in a large sized agate mortar and white thoroughly stirring, calcium cyanamide 40 g (0.50 mol) is slowly added and the mixture is grounded. Acetylene gas is generated, yielding a dull grayish to dark colored paste. Subsequently, the paste is dried at 40~50 ℃ for 12~18 hours under reduced pressure 30 mmHg to yield a gray powder which is placed in a Soxhlet extractor. The powder is extracted with 400 mL of ether containing several drops of dilute acetic acid for 2~3 hours (2×). The ether extraction is dried over anhydrous sodium sulfate (30 g). Concentration under a reduced pressure gives 10.5~15.8 g (50~75% from CaCN2) colorless viscous oil.
References
- Org. Synth. 1963, Coll. Vol. 4, 645.
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