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CAS RN: 7119-95-1 | Product Number: N0965
1-Nitropyrazole
×
Purity: >97.0%(GC)
Synonyms:
Product Documents:
| Size | Unit Price | Philadelphia, PA | Portland, OR | Japan* | Quantity |
Shipping Information
|
|---|---|---|---|---|---|---|
| 5G |
$86.00
|
3 | 1 | 8 |
|
|
| 25G |
$256.00
|
1 | 3 | 20 |
|
* Items in stock locally typically ship the same day of ordering. Items from Japan stock are able to ship from a US warehouse within 2 weeks after ordering. For additional estimated shipment times, please refer to the Shipping Simulation tool. Note: Excludes regulated items and items that ship on ice.
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| Product Number | N0965 |
Purity / Analysis Method 
|
>97.0%(GC) |
| Molecular Formula / Molecular Weight | C__3H__3N__3O__2 = 113.08 |
| Physical State (20 deg.C) | Solid |
| Storage Temperature
|
Room Temperature (Recommended in a cool and dark place, <15°C) |
| CAS RN | 7119-95-1 |
| Reaxys Registry Number | 111934 |
| PubChem Substance ID | 354334206 |
| MDL Number | MFCD00015894 |
Specifications
| Appearance | White to Light yellow powder to crystal |
| Purity(GC) | min. 97.0 % |
| Melting point | 92.0 to 96.0 °C |
| NMR | confirm to structure |
Properties (reference)
| Melting Point | 94 °C |
GHS
| Pictogram |
|
| Signal Word | Warning |
| Hazard Statements | H302 : Harmful if swallowed. H315 : Causes skin irritation. H319 : Causes serious eye irritation. |
| Precautionary Statements | P501 : Dispose of contents/ container to an approved waste disposal plant. P270 : Do not eat, drink or smoke when using this product. P264 : Wash skin thoroughly after handling. P280 : Wear protective gloves/ eye protection/ face protection. P337 + P313 : If eye irritation persists: Get medical advice/ attention. P305 + P351 + P338 : IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. P302 + P352 : IF ON SKIN: Wash with plenty of soap and water. P332 + P313 : If skin irritation occurs: Get medical advice/ attention. P362 : Take off contaminated clothing and wash before reuse. P301 + P312 + P330 : IF SWALLOWED: Call a POISON CENTER/doctor if you feel unwell. Rinse mouth. |
Related Laws:
Transport Information:
| HS Number | 2933.19.9000 |
Application
ニトロ化剤
Experimental procedure: Toluene (9.2 g, 0.1 mol) and 1-nitropyrazole (1.14 g, 0.01 mol) are dissolved in dichloromethane (50 mL). Into this solution, a solution of triflic acid (0.75 g, 0.01 mol) in dichloromethane (10 mL) is added. The reaction mixture is vigorously stirred at 25 °C under a dry nitrogen atmosphere. After 10 h the reaction mixture is quenched with ice-water and extracted with ether (2 x 50 mL). The ethereal extract is washed with sodium bicarbonate solution (5%, 25 mL) and brine and dried over anhydrous MgSO4. The ether is evaporated and the residue distilled to yield a mixture of nitrotoluenes (1.16 g, 92%).
References
- Aromatic Substitution. 47. Acid-Catalyzed Transfer Nitration of Aromatics with N-Nitropyrazole, a Convenient New Nitrating Agent
PubMed Literature
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