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CAS RN: 35109-88-7 | Product Number: I0759
2-Iodoadenosine
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Purity: >98.0%(HPLC)(N)
Synonyms:
- 6-Amino-2-iodo-9-(β-D-ribofuranosyl)purine
Product Documents:
| Size | Unit Price | Philadelphia, PA | Portland, OR | Japan* | Quantity |
|---|---|---|---|---|---|
| 200MG |
$86.00
|
3 | 1 | 5 |
|
| 1G |
$337.00
|
3 | 2 | 18 |
|
| 5G |
$842.00
|
2 | 1 | 3 |
|
* Items in stock locally ship in 1-2 business days. Items from Japan stock are able to ship from a US warehouse within 2 weeks. Please contact TCI for lead times on items not in stock. Excludes regulated items and items that ship on ice.
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| Product Number | I0759 |
| Purity / Analysis Method | >98.0%(HPLC)(N) |
| Molecular Formula / Molecular Weight | C__1__0H__1__2IN__5O__4 = 393.14 |
| Physical State (20 deg.C) | Solid |
| Storage Temperature | Room Temperature (Recommended in a cool and dark place, <15°C) |
| CAS RN | 35109-88-7 |
| Reaxys Registry Number | 4546706 |
| PubChem Substance ID | 87561674 |
| MDL Number | MFCD01320413 |
Specifications
| Appearance | White to Orange to Green powder to crystal |
| Purity(HPLC) | min. 98.0 area% |
| Purity(with Total Nitrogen) | min. 98.0 % |
| NMR | confirm to structure |
Properties (reference)
| Melting Point | 144 °C |
| Maximum Absorption Wavelength | 265(H2O) nm |
GHS
Related Laws:
Transport Information:
| HS Number | 2934.99.4400 |
Application
Palladium-catalyzed cross-coupling reaction with terminal alkynes
Typical procedure: 2-Iodoadenosine (393 mg), CuI (9.5 mg), bis(triphenylphosphine)palladium(II) dichloride (36 mg), triethylamine (0.16 mL) and ethynylbenzene (123 mg) in DMF (7 mL) is heated 80 °C for 1 h. After 2-iodoadenosine is completely consumed, the reaction mixture is concentrated to dryness under reduce pressure. The residue is dissolved in CHCl3, and H2S gas is introduced to the solution (~30 s) followed by N2 gas. The suspension is filtered through a Celite pad and washed with CHCl3. The combined filtrate is concentrated to dryness in vacuo, and the residue is purified by a silica gel column chromatography (eluent: MeOH–CHCl3) to give 2-(phenylethyn-1-yl)adenosine (373 mg, 97 %).
References
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