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Published TCIMAIL newest issue No.197
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CAS RN: 10416-59-8 | Product Number: B0911
N,O-Bis(trimethylsilyl)acetamide Kit BSA 1 mL × 8 / Reaction vial, capacity 2 mL × 8
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Purity: >80.0%(GC)
Synonyms:
- BSA Kit
Product Documents:
| Size | Unit Price | Belgium | Japan* | Quantity |
|---|---|---|---|---|
| 1KIT |
€73.00
|
1 | 15 |
|
*Stock available in Belgium will be delivered in 1 to 3 days
*Stock available in Japan will be delivered in 1 to 2 weeks (excludes regulated items and dry ice shipments).
| Product Number | B0911 |
| Purity / Analysis Method | >80.0%(GC) |
| Physical State (20 deg.C) | Liquid |
| Storage Temperature | Room Temperature (Recommended in a cool and dark place, <15°C) |
| Store Under Inert Gas | Store under inert gas |
| Condition to Avoid | Moisture Sensitive |
| Packaging and Container | 1KIT-Vial (View image) |
| CAS RN | 10416-59-8 |
| Reaxys Registry Number | 1306669 |
| PubChem Substance ID | 87563876 |
| MDL Number | MFCD00008270 |
Specifications
| Appearance | Colorless to Light yellow clear liquid |
| Purity(GC) | min. 80.0 % |
| High boiling impurity of Silylation agent | No impurity higher than Isopropyl myristate(50 ppm) after 5 min + hold up time |
Properties (reference)
| Melting Point | -24 °C |
| Boiling Point | 73 °C/35 mmHg |
| Flash point | 42 °C |
| Specific Gravity (20/20) | 0.83 |
| Solubility (soluble in) | Ether, Benzene, dichloromethane |
GHS
| Pictogram |
|
| Signal Word | Danger |
| Hazard Statements | H302 : Harmful if swallowed. H314 : Causes severe skin burns and eye damage. H226 : Flammable liquid and vapour. |
| Precautionary Statements | P210 : Keep away from heat, hot surfaces, sparks, open flames and other ignition sources. No smoking. P280 : Wear protective gloves/ protective clothing/ eye protection/ face protection/ hearing protection. P370 + P378 : In case of fire: Use dry sand, dry chemical or alcohol-resistant foam to extinguish. P303 + P361 + P353 : IF ON SKIN (or hair): Take off immediately all contaminated clothing. Rinse skin with water. P304 + P340 + P310 : IF INHALED: Remove person to fresh air and keep comfortable for breathing. Immediately call a POISON CENTER/doctor. P305 + P351 + P338 + P310 : IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. Immediately call a POISON CENTER/doctor. |
Related Laws:
| EC Number | 233-892-7 |
| RTECS# | AK3000000 |
Transport Information:
| UN Number | UN2920 |
| Class | 8 / 3 |
| Packing Group | II |
| HS Number | 2931900090 |
Application
Trimethylsilylating Reagent for GC Derivatization
Experimental procedure:BSA is added to a sample (10-50 mg) placed into a dry vessel, and the vessel is sealed tightly. If necessary, it is heated at 70-80 °C for 30 min - 1 h.
References
- Quantitative gas-liquid chromatography of sulfur containing amino acids
Application
Reactivity of Trimethylsilylating Reagents : Trimethylsilylation of Alcohols
References
- Protection for the Hydroxyl Group, Including 1,2- and 1,3-Diols
- P. G. M. Wuts, in Greene’s Protective Groups in Organic Synthesis, 5th ed., ed. by P. G. M. Wuts, John Wiley & Sons, Inc., Hoboken, New Jersey, 2014, Chap. 2, 17.
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